Advances in atomic spectroscopy. / Volume 2 - download pdf or read online

By J. Sneddon

ISBN-10: 0080546374

ISBN-13: 9780080546377

ISBN-10: 1281026816

ISBN-13: 9781281026811

This sequence describes chosen advances within the zone of atomic spectroscopy. it really is promarily meant for the reader who has a historical past in atmoic spectroscopy; appropriate to the amateur and professional. even though a familiar and permitted technique for steel and non-metal research in a number of advanced samples, Advances in Atomic Spectroscopy covers quite a lot of fabrics. every one bankruptcy will thoroughly conceal a space of atomic spectroscopy the place swift improvement has occurred.

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This recent work indicates that background correction for LEAFS may require measurement of the background signal with a more accurate and precise method than off-line measurements. Several instrumental approaches to background correction for graphite furnace LEAFS have been investigated that include (1) multichannel correction techniques, (2) wavelength background correction and, (3) Zeeman background correction. A. Multichannel Background Correction Techniques Sjtistrt~m (1990a) described a multichannel background correction technique for graphite furnace LEAFS that used three optical fibers located at the exit slit of the monochromator.

1993). (continued) 29 30 DAVID J. BUTCHER o 80C 0 11) (b) 60 0 m :: 40 i,1,,, 11) > = m m mr' 20 0 . . i - - i . 74 . . I . . . . 80 Excitation wavelength, nm Figure 15. (continued) advantage that background correction was made simultaneously with the signal measurement, both signal and background being measured with every laser pulse. Second, this technique can be employed with any atom cell because it involves modification of the detection system. Third, this multichannel method can be used with any laser repetition rate.

BACKGROUND CORRECTION FOR LEAFS Butcher et al. (1988) reviewed the types of background present in graphite furnace LEAFS. These include blackbody emission, laser scatter, molecular fluorescence, and nonanalyte atomic fluorescence. Blackbody emission and laser scatter can be 26 DAVID J. BUTCHER described as broadband background signals, whose magnitude does not vary near the atomic line. Molecular fluorescence and nonanalyte atomic fluorescence may give a structured background whose magnitude changes with wavelength.

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Advances in atomic spectroscopy. / Volume 2 by J. Sneddon


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