By C.M. Rayner
This quantity is a testomony to the ongoing significance of sulfur chemistry, and the great growth that has been made lately.
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Extra resources for Advances in Sulfur Chemistry, Volume 2
J. Chem. Soc, Perkin Trans. 1 1993, 1011. 10. Bonini, B. ; Zani, P. Synthesis 1995, 92. 11. ; Seconi, G. J. Org. Chem. 1988,55,3612. 12. Brillon, D. Sulfur Rep. 1992,12, 297. 13. ; Bonini, B. ; Zani, R J. Chem. Soc, Perkin Trans. 11986, 381. 14. ; Bonini, B. ; Zani, P. J. Org. Chem. 1990, 55, 3744. 15. ; Benaglia, M. J. Organomet. Chem. 1992,434, 151. 16. Bonini, B. ; Zani, R; Maccagnani, G. J. Chem. Soc, Perkin Trans. 1 1989, 2083. 17. Bonini, B. ; Zani, R J. Chem. Soc, Chem. Commun. 1988, 365.
By slowly adding the enethiol to a suspension of solid sodium hydroxide or cesium carbonate in diethyl ether (Scheme 32). In this way^^'^^ the compounds with the 8- (n = 5), 12- (n = 9) and 14- (n = 11) membered rings were synthesized in good yields. C. Synthesis of Open-Chain a-Silyl Vinyl Sulfides The simplest compound in this series, 1-phenylthio-l-trimethylsilyl ethylene 45, was conveniently prepared by Magnus and co-workers either by reaction of a-lithio vinyl phenyl sulfide 46 with trimethylsilylchloride,^^ or by addition of arylsulfeny 1chloride to vinyl trimethylsilane followed by elimination of hydrogen chloride^^ (Scheme 33).
J. Chem. Soc, Perkin Trans 11985, 1115. 65. (a) Chan, T. ; Mychajlowskij, W. Tetrahedron Utt. 1974, 3479; (b) Chan, T. ; Lau, R W. , Li, M. R Tetrahedron Lett. 1976, 2667. 66. ; Nozaki, H. Tetrahedron Lett. 1983, 24, 2877. 67. ; McLachlan, A. D. Introduction to Magnetic Resonance, Harper & Row: New York, 1969; (b) Wertz, J. ; Bolton, J. R. Electron Spin Resonance: Elementary Theory and Practical Applications, McGraw-Hill: New York, 1972. 68. Perkins, M. J. ; Academic Press: London, 1980, Vol. 17, p.
Advances in Sulfur Chemistry, Volume 2 by C.M. Rayner